Agilent Technologies Agilent G1369B Manual de usuario Pagina 18
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18 Agilent 1260 Infinity High Performance Autosampler User Manual
1 Introduction
Autosampler Principle
Inject-and-Run The final step is the inject- and- run step. The six- port valve is switched to
the main- pass position, and directs the flow back through the sample
loop, which now contains a certain amount of sample. The solvent flow
transports the sample onto the column, and separation begins. This is the
beginning of a run within an analysis. In this stage, all major
performance- influencing hardware is flushed internally by the solvent
flow. For standard applications no additional flushing procedure is
required.
Figure 5 Inject and Run
- Agilent 1260 Infinity 1
- High Performance 1
- Autosampler 1
- In This Guide 3
- Contents 5
- Features 10
- Overview of the Module 11
- 1 Introduction 12
- Autosampler Principle 13
- Injection Sequence 14
- System Overview 19
- Agilent Technologies 23
- Site Requirements 24
- Power Cords 25
- Bench Space 26
- Condensation 26
- Physical Specifications 27
- Specifications 28
- Installing the Autosampler 31
- Unpacking the Autosampler 32
- Delivery Checklist 33
- 3 Installing the Autosampler 34
- One Stack Configuration 36
- Two Stack Configuration 38
- Using the Module 47
- Leak and Waste Handling 48
- Preparing the Autosampler 49
- 4 Using the Module 50
- & 53
- ' 53
- Control Settings 55
- Method Parameter Settings 56
- Module Configuration 60
- (G4208A) 61
- Optimizing Performance 65
- Delay Volume 66
- 5 Optimizing Performance 68
- Status Indicators 80
- Error Messages 80
- Module Status Indicator 82
- User Interfaces 83
- Agilent Lab Advisor Software 84
- Error Information 85
- 7 Error Information 86
- What are Error Messages 87
- General Error Messages 88
- Remote Timeout 89
- Lost CAN Partner 89
- Leak Sensor Open 90
- Leak Sensor Short 91
- Compensation Sensor Open 91
- Compensation Sensor Short 92
- Fan Failed 92
- Module Error Messages 93
- Side Door Error 94
- Valve to Bypass Failed 95
- Valve to Mainpass Failed 95
- Needle Lock Failed 96
- Needle Carrier Failed 97
- Initialization Failed 99
- Metering Home Failed 100
- Motor Temperature 101
- Invalid Vial Position 102
- Peristaltic Pump Error 103
- Vessel or Wash Vessel Error 103
- Vessel Stuck to Needle 104
- Rear Blind Seat Missing 104
- Test Functions 105
- Introduction 106
- System Pressure Test 107
- 8 Test Functions 108
- Maintenance Positions 112
- Change Needle 113
- Change Loop Capillary 113
- Arm Position 114
- Change Needle Carrier 114
- Change Metering Device 115
- Injector Steps 116
- Step Commands 117
- Maintenance 119
- Introduction to Maintenance 120
- Warnings and Cautions 121
- Overview of Maintenance 122
- Cleaning the module 123
- Removing the needle assembly 124
- 9 Maintenance 126
- Exchanging the Needle Seat 130
- Replacing the Rotor seal 132
- Removing the Metering Seal 135
- >chZgiidda 137
- Tools required Description 143
- Flat head screwdriver 143
- Parts required # Description 143
- 1 Interface board 143
- Replacing the Module Firmware 144
- Parts for Maintenance 145
- 10 Parts for Maintenance 146
- Vial Trays 147
- Recommended Vial Plates 149
- Accessory Kit 150
- Injection Ugrade Kit 150
- Analytical Head Assembly 151
- Injection Valve Assembly 152
- Cover Parts 153
- Leak System Parts 154
- Identifying Cables 155
- Cable Overview 156
- Analog Cables 158
- Remote Cables 160
- 11 Identifying Cables 162
- BCD Cables 163
- CAN/LAN Cables 165
- External Contact Cable 166
- Agilent Module to PC 167
- Hardware Information 169
- Firmware Description 170
- GZh^YZciHnhiZb 171
- BV^c;LjeYViZ 171
- BV^cHnhiZb 171
- GZh^YZci;LJeYViZ 171
- 12 Hardware Information 172
- Obstruction of transport unit 173
- Electrical Connections 174
- Rear view of the module 175
- Interfaces 176
- Overview Interfaces 179
- >chigjbZci 180
- BVaZ ;ZbVaZ ;ZbVaZ BVaZ 180
- APG Remote 181
- Special Interfaces 182
- Special Settings 186
- Instrument Layout 187
- Early Maintenance Feedback 188
- LAN Configuration 189
- 13 LAN Configuration 190
- Connecting the module via LAN 191
- Appendix 193
- General Safety Information 194
- Operation 195
- Safety Symbols 196
- Lithium Batteries Information 197
- (2002/96/EC) 198
- Radio Interference 199
- Sound Emission 200
- Use of Solvents 201
- 14 Appendix 202
- *G1367-90014* 206
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