Agilent Technologies 1100 Series Manual de instrucciones Pagina 28
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18 1100 Series Capillary LC System Manual
1 Installing your Capillary LC System
Install the Diode Array Detector (DAD) (G1315B)
1 Ensure the line power switch at the front of the diode array detector DAD is
off.
2 If the system is to be connected to the user interface by LAN, install the
JetDirect card into the DAD. See Replacing the Interface Board in the DAD
Reference Manual.
3 Place the DAD on top of the TCC. Make sure that the two modules are
interlocked correctly.
4 Connect one end of the LAN cross over cable (5183-4649) to the connector
on the JetDirect card. Connect the other end of the LAN cross over cable to
the Chemstation.
5 Connect the free end of CAN-bus cable (5181-1516) from the TCC to one of
the CAN connectors at the rear of the DAD.
6 Connect the power cable to the power socket at the rear of the DAD. Do not
connect the power cable to power until you have finished the hardware
installation of all modules in the stack.
7 Install the DAD flow cell (G1314-68714).
8 Route the DAD flow cell outlet capillary (G1315-68708) to an appropriate
waste container.
9 Connect The DAD flow cell inlet capillary (G1315-68703) to the outlet of the
analytical column.
Ccarefully route all capill aries so that they are not c rushed or b roken by module front covers. Avoid ex cessive bending. S ee chapter 2 for advice on handli ng capillaries.
WARNING
Connect the power cable to power only after you have finished the hardware
installation of all modules in the stack.
NOTE
Carefully route all capillaries so that they are not crushed or broken by module front covers.
Avoid excessive bending. See Chapter 2 for advice on handling capillaries.
- Agilent 1100 Series 1
- Capillary LC System 1
- In This Manual… 3
- Contents 5
- Agilent Technologies 11
- Site Requirements 12
- Bench Space 13
- Environment 13
- Physical Specifications 14
- System Installation Process 16
- Install the Solvent Cabinet 23
- Micro Well-plate Sampler) 26
- Purging the Pump 34
- Inject the Check-out Sample 36
- Procedure 37
- Optimizing Performance 39
- Pump issues 40
- Fused Silica Capillary issues 41
- Sampler issues 42
- Column thermostat issues 42
- DAD issues 42
- Cleaning the Solvent Filters 45
- When to use Alternative Seals 47
- Static Mixer and Filter 50
- How the Function Works 53
- Capillaries and Fittings 55
- Capillary Flow Diagram 56
- Capillaries and Fittings 3 57
- * 2.2 12 5065-9906 61
- * 1.4 7.6 G1375-87313 61
- Fittings and Ferrules 62
- Basic System Troubleshooting 65
- Symptoms: 66
- Poor peak shape 71
- Wandering Detector Baseline 73
- Parts and Materials 75
- Micro Vacuum Degasser 76
- Capillary Pump 79
- Capillary Pump Hydraulic Path 82
- Pump-Head Assembly 84
- Figure 9 Pump head assembly 85
- Capillary pump cover parts 86
- Micro Well-plate Sampler 87
- Thermostat for 1100 Samplers 98
- 5 Parts and Materials 100
- Parts and Materials 5 101
- Vial Trays 104
- Micro Column Switching Valve 107
- Diode Array Detector 111
- DAD - Optical Unit Assembly 113
- Figure 30 Optical Unit Parts 114
- 500 nl Flow Cell 115
- Fan Assembly Parts 117
- Holmium Oxide Filter 118
- Common Parts 120
- Rear panel 121
- Power and Status Light Pipes 122
- Leak Parts 123
- Foam parts 124
- Sheet metal kit 124
- Micro Degasser Accessory Kit 125
- Capillary Pump Accessory Kit 126
- G1316-68725 129
- DAD Accessory Kit 130
- Tabl e 61 Cables overview 131
- Analog Cables 133
- Remote Cables 134
- BCD Cables 140
- Auxiliary Cable 142
- CAN Cable 142
- External Contact Cable 143
- RS-232 Cable Kit 144
- LAN Cables 144
- Options 6 147
- 6Options 152
- Frequency If valve leaks 156
- 9/64 inch hex key 156
- • Disconnect the power cable 157
- • Disconnect capillaries 157
- Features 163
- Performance Specification 163
- Installation of the Flow Cell 166
- ~ 0.3 mm clearance 167
- Replacing or Cleaning Parts 171
- Performance Specifications 175
- 7 Performance Specifications 176
- Performance Specifications 7 177
- Autosampler 179
- Compartment 181
- Safety Information 185
- Operation 186
- Safety Symbols 187
- Lithium Batteries Information 188
- Danish Information: 188
- Radio Interference 189
- Sound Emission 189
- Solvent Information 189
- ' %%(&' 196
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