Agilent Technologies 8000 Series Manual del operador Pagina 101

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Operating the 8000 4
8000 Operator’s Manual 101
Checking the Calibration - Volume Accuracy
Check the calibration by running a short sampling procedure and
dispensing the requested volume into calibrated test tubes:
1 Place an appropriate number of 10 mL calibration tubes in row 9 of
the 8000 sample tray.
2 Ensure the sample cannulas of the dissolution apparatus are
sufficiently submerged in water.
3 From the Ready screen, press MANUAL SAMPLE.
4 Enter the following parameters:
5 Verify the values for each parameter which are shown at the bottom
of the display screen for this manual program.
6 If the values are correct, select option 1, Start, to start the sampling
procedure. The 8000 dispenses 10 mL into the calibration tubes in
row 9 of the sample tray.
7 Check the volume in each tube to ensure the 8000 is dispensing
10 mL ± 0.5 mL from each position.
8 If the volumes are not correct, repeat the calibration of the 8000
according to the procedure described under “Automatic
Calibration” on page 97 as appropriate.
If the volumes are correct, you are ready to use the 8000 to collect
samples.
Table 2 6 Volume Accuracy Parameter Options
Selection Response
2 Set Row # Enter 9 and press ENTER.
3 Set Volume Enter 10 and press ENTER.
4 Prime Time Enter 60 and press ENTER.
5 Purge Time Enter 60 and press ENTER.
6 RM Option Ensure the RM option is disabled.
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