Agilent Technologies 8000 Series Manual del operador Pagina 97

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Operating the 8000 4
8000 Operator’s Manual 97
Volumetric Calibration (Peristaltic Pump only)
It is critical that sample volumes are accurately and precisely taken.
Calibration of your system ensures this by recording in memory the time
required to deliver a nominal 10 mL of medium into the graduated
calibration tubes. Refer to “Automatic Calibration” below or “Manual
Calibration” on page 99 for specific operating procedures necessary to
calibrate your 8000.
Automatic Calibration
To perform automatic calibration, complete the following steps:
1 Ensure the sample cannulas of the dissolution apparatus are
sufficiently submerged in water.
2 Ensure the correct prime and purge times have been entered via the
Main Menu options 4 and 5, Manual Prime Time and Manual Purge
Time, respectively.
3 Ensure the supplied autocalibration block is firmly in place and
connected to the rear panel jack labeled AUTO CALIBRATION.
4 From the Ready screen, press CAL. The dispensing arm moves
forward to allow you to check the autocalibration block.
NOTE
The CAL key on the 8000 can be used only if the peristaltic pump is
installed on your system. To calibrate the syringes in the 806 Syringe
Pump, see “5 Full Stroke (hidden option)” under “Main Menu Option 3
- Set Syringe Pump” on page 80“.
NOTE
Ensure the cannula filters are in place during calibration.
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